PPL LINED HYDROTHERMAL AUTOCLAVE (SAFE TEMP – 260°C)

PPL LINED HYDROTHERMAL AUTOCLAVE (SAFE TEMP – 260°C)

 15,900.00 88,900.00

In stock

 15,900.00 88,900.00

SKU: AUTO-PPL Category:
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Additional information

WeightN/A
Capacity

25, 50, 100, 150, 200, 250, 500

Reactor Sealing Type

Screw Sealing

Safe Temperature

260°C

Max Operating Temperature

280°C

Working Pressure

≤ 3MPa

Heating and Cooling Rate

≤5°C/min

Outer Shell Material

Stainless steel (SS-304)

Inner Shell Material

PPL

Pressure Gauge

No

  • Place the Autoclave and sterilizing material on the table or on the shelf.
  • Twist the screw type threaded primary SS cap (SS Alloy 304) in an anticlockwise direction until it has been opened.
  • There is 2 type of SS gasket/lid in the reactor, 1 is on the bottom side and another is on top of the Teflon vessel chamber.
  • Lift the top SS gasket or lid and take-out milky white colorPTFE/Teflon reaction chamber.
  • Now fill solvent (as per liner’s capacity) in the reaction chamber and sealed it.
  • Make sure that the Teflon cap should be air-tight to avoid pressure leakage.
  • Place Teflon or PTFE liner in a stainless steel chamber.
  • Keep top gasket over the vessel and make sure that the Teflon-lined vessel placed properly inthe Stainless Steel chamber.
  • Then twist primary SS cap in a clockwise direction until it does not turn anymore.
  • The secondary SS cap has been given at the top of the primary cap for extra tightening to avoid pressure leakages.
  • Rotate primarySS cap in the clockwise direction with the help of locking rod for additional tightening.
  • Placed the hydrothermal autoclave in oven or furnace and heat it till reactor’s safe temperature.
  • Increase the temperature of the oven and set heating rate5 0C/minute only.
  • A researcher can heat the hydrothermal autoclave till 200 0C for safe use.
  • After completion of the hydrothermal synthesis reaction, the autoclave’s cooling rate will be 5 0C/minute.
  • Make sure that, after completion of the process clean PTFEor Teflonliner properly for reuse.
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